Region 1 from 9.210 to 9.077 ppm T1 = 18.367s Region 2 from 8.807 to 8.691 ppm T1 = 11.364s Region 3 from 8.497 to 8.378 ppm T1 = 9.607s Region 4 from 7.656 to 7.522 ppm T1 = 6.466s